By Pradyot Patnaik
This crucial on-the-job source for the analytical chemist has been revised and up-to-date with forty% new fabric. Readers will locate the entire traditional rainy and instrumental suggestions in a single exhaustive reference in addition to the entire serious info had to observe them. labored examples, troubleshooting assistance, and diverse tables and charts are supplied for simple entry to the knowledge.
* the main updated and entire advisor to analytical chemistry on hand at the present time
* NEW: three significant chapters on research of Indoor Air, research of insecticides, research of hint Metals
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Pap. answer; eluted 501-D:131 (1964) with 1 M H SO 2 four Titanium Dowex 50-X8 Adsorbed from Al, Be, Cd, Co, Cu, F. W. E. Strelow, Anal. Chem. <0. three M acid Fe(III), los angeles, Mg, Mn, 35:1279 (1963) answer; Ti eluted Ni, Sc, Th, Th, Y, with zero. five M and Zn H SO −1% H O 2 four 2 2 Dowex four different metals eluted Al, Cr(III), Cu, Ga, R. Kuroda et al. , Anal. Chim. Acta with zero. 1 M lanthanoids, and Mg 62:343 (1972) H SO −0. 15% 2 four H O , then Ti 2 2 with 2 M H SO 2 four Dowex 1 Adsorbed from 1 M Biomaterials and T. Kiriyama et al. , Z. Anal. Chem. NH SCN−1 M seawater 307:352 (1981); 313:328 (1982) four HCl, eluted with four M HCl Tungsten Dowex 50 zero. 1 M HCl plus low Bivalent metals G. Gottschalk, Z. Anal. Chem. focus of 187:164 (1962) oxalic acid; W now not adsorbed Dowex 50-X8 Elute W with Fe(III) and Ga A. R. Eberle, Anal. Chem. zero. 084 M HF 35:669 (1963) Dowex 1-X8 Adsorbed from Al, Cu, Fe(III), Ni, T. Shimizu et al. , Jpn. Anal. zero. 07 M (NH ) SO – Sc, Th, U(VI), 15:120 (1966) four 2 four zero. 025 M H SO ; V(IV), Zn, and Zr 2 four W eluted with zero. five M NaCl−0. five M NaOH Uranium(VI) Dowex 50 U retained from As(III), Co, Cr(III), V. Pekarek and S. Maryska, 1 M HClO and Cu, Mn(II), Mo(VI), gather. Czech Chem. Commum. four eluted with 1 M W(VI), V(V), 33:1612 (1968) HCl and Zn Dowex 50 U eluted with 1 M HCl Thorium and S. M. Khopkar and A. okay. De, Anal. phosphate Chim. Acta 22:153 (1960) Downloaded from electronic Engineering Library @ McGraw-Hill (www. digitalengineeringlibrary. com) Copyright © 2004 The McGraw-Hill businesses. All rights reserved. Any use is topic to the phrases of Use as given on the web site. initial SEPARATION equipment initial SEPARATION equipment 2. 89 desk 2. 38 chosen functions of Ion alternate for the Separation of a selected point from different parts or Ions ( endured ) aspect Resin section Aqueous part Separated from Reference Uranium Dowex 50W-X8 U eluted with zero. 1 M Bi, Fe(III), Pb, Zn J. S. Fritz, B. B. Garralda, and HF S. ok. Karraker, Anal. Chem. 33:882 (1961) Dowex 50W-X8 U eluted with Cd, Co, l. a., Mg, J. S. Fritz and T. A. Palmer, Talanta sulfosalicylic acid and Ni 9:393 (1967) at pH 6–7; different metals retained Dowex 1 U adsorbed from Ca, Ce, Fe(III), and Th F. Hecht et al. , Mikrochim. acetate medium at Acta 1956:1283 pH four. 3−5. 2 and eluted with zero. eight M HCl Dowex 1 U adsorbed from Al, Co, Cr, Fe, J. Korkisch, A. Farag, and F. ascorbic acid lanthanoids, Mn, Ni, Mikrochim. Acta 1958:415; answer at pH and Pb 1959:693 four. 0−4. five, then eluted with 1 M HCl Vanadium Dowex 1 zero. 1 M HCl–0. 1 M Biomaterials and T. Kiriyama and R. Kuroda, Anal. NH SCN seawater Chim. Acta 62:464 (1972); four Analyst 107:505 (1982); Mikrochim. Acta 1985:(I) 405; Chromatographia 21:12 (1986) Vanadium(IV) Dowex 1 12 M HCl Fe(III) and Ti ok. A. Kraus, F. Nelson, and G. W. Smith, J. Phys. Chem. 58:11 (1954); C. Michaelis et al. , Anal. Chem. 34:1764 (1962) Zinc Dowex 1 zero. 1 M HCl plus Al, alkaline earth S. Kallmann, C. G. Steele, 10% NaCl metals, Be, Cd, Co, and N.
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